In-Situ Raman Spectroscopy of Single Microparticle Li-Intercalation Electrodes
Modifications in the vibrational properties of a single microparticle of LiMn2O4 induced by extraction and subsequent injection of Li(+) into the lattice have been monitored in situ via simultaneous acquisition of Raman scattering spectra and cyclic voltammetry data in 1M LiC1O4 solutions in ethylene carbonate (EC): diethyl carbonate (DEC) mixtures (1:1 by volume). Statistical analyses of the spectra in the range 15
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